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Mesoporous silica of SBA-15 kind was modified for the first time with 3-(trihydroxysiyl)-1-propanesulfonic acid (TPS) by post-synthesis modification involving microwave or standard heating with the intention to generate the BrÃ¸nsted acidic centers on the material floor. The samples structure and composition have been examined by low temperature N2 adsorption/desorption, XRD, HRTEM, elemental and thermal analyses. The floor properties have been evaluated by esterification of acetic acid with n-hexanol used as the check reaction. A much increased efficiency of TPS species incorporation was reached with the appliance of microwave radiation for 1 h than typical modification for 24 h. It was found that the structure of mesoporous help was preserved after modification using each methods applied on this study. Materials obtained with the use of microwave radiation showed a superior catalytic activity and high stability. Working on a manuscript? The construction of those solids is characterized by comparatively giant floor area, e.g. 1000 m2 gâˆ’1, and the presence of hexagonal channels regular in size.